how to manufacture the d enantiomer of phenylaminopropane and 34methylenedioxymethphenylaminopropane
Title: how to manufacture the d enantiomer of phenylaminopropane and 34methylenedioxymethphenylaminopropane
Category: /Law & Government/Government & Politics
Details: Words: 10881 | Pages: 40 (approximately 235 words/page)
how to manufacture the d enantiomer of phenylaminopropane and 34methylenedioxymethphenylaminopropane
Category: /Law & Government/Government & Politics
Details: Words: 10881 | Pages: 40 (approximately 235 words/page)
Re: DETAILED METHODS for NON-CHEMISTS
METHamphetamine PRECURSS CLEANING/wkUP
Extractomania........by Ozbee friends..........edited by Placebo
INDEX:
1: Equipment
2: Ingredients
3: Method
step 1:
step 2:
step 3:
step 4:
step 5:
step 6:
4: Acid/Base
5: HCl-Gassing
6: Notes
1: Equipment
* Various jars, glass vessels, beakers etc
* PH paper, electronic PH tester
* Filter paper coffeee filters
* A strainer that will fit your filters nicely,
so that you get better surface area then a funnel
* Hair dryer, heat lamps
* Hot plate, no open flames, only heat
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pure 2CB x HCl as a white crystaline solid.
Yield - 34.0g (57%) of 2CB Hydrochloride.
Purity - Single spot by TLC. NMR is clean.
I have references for the two reduction steps and the bromination, but can't seem to find them. If someone asks really nicely I might be persuaded to find and post them.
Also, before some jackass reads this procedure and asks me why 4 eq.of sodium borohydride is used for the reduct